The obtained residue was reconstituted with acetonitrilewater 3. Available floor area is sufficient and flooring will support the load. Why lchighresolutionms will become a key instrument in clinical labs. Switchable between gcms and lcms mass range up to mz3000 scan speeds. Get screencastify simple screen video recording for chrome. This is of significant value when analyzing multiple classes of compounds in one sample that require ionization in both polarities. Pdf from targeted quantification to untargeted metabolomics. Attachments thermo scientific tsq quantum xls and tsq quantum gc preinstallation requirements guide 2 mb. An ultra performance liquid chromatographtandem mass spectrometer uplcmsms was used to identify nas in the collected air samples, as described below. Quantum unit of spin definition of quantum unit of spin by. Preface the thermo scientific tsq quantum xls and tsq quantum xls ultra systems make up the tsq quantum xls series and are member of the tsq quantum family of mass spectrometers. It is a windows application and it runs on both 32bit and 64bit. Quantum supports customer efforts to backup, replicate and archive data in cloud locations. Stateoftheart electronics and comprehensive diagnostics are hallmarks of our instruments.
For each qcloud offering quantum provides support to ensure successful customer cloud operations. It has the ability to do 3000 timed srms as well as triggering datadependent full scan msms quantitationenhanced datadependent msms qedmsms giving the multicomponent screening experiment an added dimension of specificity. Sep 20, 2011 new gctriple with ultra selective reaction monitoring. Low voltage directive 200695ec this device complies with low voltage directive 200695ec and harmonized standards. Thermo scientific pierce triple quadrupole calibration. It features the revolutionary product specifications thermo scienti. Shiseido, tokyo, japan coupled to a mass spectrometer tsq quantum ultratm triple quadrupole, thermo fisher scientific, waltham, usa. Low voltage safety compliance this device complies with european union directive 200695ec implemented by 610101. Tsq quantum is more twice higher sensitivity than tsq vantage. For research use only not for use in diagnostic procedures tsq quantum gc user guide 7011197151 revision a september 2007. Compatible mass spectrometers tsq access max tsq quantum discovery tsq quantum ultra tsq vantage tsq endura tsq quantiva creating. Analysis of microcystins from bluegreen algae using the tsq quantum ultra lcmsms system be the first to rate this application. There may be a problem with the power entry module.
The thermo scientific tsq quantum access max triple quadrupole mass spectrometer is. This acquisition mode is known as ultraselective reaction. The maxtor fireball cr was developed by quantum corporation prior to its merger with maxtor. Compared to other triple quadrupole instruments, the tsq is unique in its design as it contains hyperbolic quadrupole rods for higher ion transmission and it also contains an slens for more thorough desolvation of ions resulting in increased signal.
Thermo forma tsq quantum ultra am accurate mass lcmsms. Ultra pdf merger is a freeware pdf utility that joins your pdf files, or part of them, together. In order to achieve the ultra ata66 transfer speed, you must have a system and a bios that will support ultra. Laboratory procedure manual centers for disease control. Overview to scale the picture below is a simulation at scale of the thermo tsq quantum ultra lcms system mass spectrometer system right side connected with a dionex uhplc left side, installed on a. Tsq quantum xls and tsq quantum gc preinstallation. Used thermo tsq quantum ultra mass spectrometer for sale. Low volume whole blood samples by lc msms utilizing turboflow methods peter ashton, alex allan, bob ardrey, triple a forensics ltd. Tsq quantum xls or tsq quantum gc system is on site. Thermo fisher scientific tsq quantum lcmsmsdemo quantum tune masteresi. Tsq quantum gc the next evolution in gcmsms systems the thermo scientific tsq quantum gc defines a new standard of excellence in gcmsms for environmental food safety, pharmaceutical, and clinical research laboratories. Tsq quantum access max emc directive 2004108eec emc compliance has been evaluated by tuv rheinland of north america, inc. Regulatory compliance thermo electron san jose performs complete testing and evaluation of its products to.
The laboratory room temperature must be maintained between 1527c 5981f. Thermofisher scientific finnigan tsq quantum discovery max. Wsi and merged them with its portfolio firm, aerometric, inc. Technical information contained in this publication is for reference purposes only and is subject to change without notice. Development of a diluteandshoot lcmsms method with 21.
Rapid analysis of opiates from low volume whole blood. Our exclusive contracts with our clients yield a wide range of used mass spectrometers from a number of respected oems, including agilent, thermo scientific, applied biosystems, waters, perkin elmer, and many more. Doorways, hallways, and so on are a minimum width of 94 cm 37 in. Acephate ap, methamidophos mmp, omethoate omet and dimethoate dmet are organophosphorus pesticides ops pesticides.
Tsq quantum xls ultra gcmsms the gold standard in highperformance gc. Keeping your timeline on track requires scientific expertise, operational experience and uptodate knowledge of the regulatory environment. Fast data acquisition rate 1 second with very high mass resolution. This system features the innovative qedmsms scan mode for unmatched sensitivity and selectivity. The tsq quantum access, a triple quadrupole mass spectrometer, offers versatility with its best in class mass range mz 303000. Design, implementation and multisite evaluation of a system. Quantum standard service and support plans quantum. Thermo electron finnigan tsq quantum ultra rensselaer. Finnigan tsq quantum ultra thermo fisher scientific. Ionbench thermo tsq quantum access max lcms system. Mergers and acquisitions purchase, sale and merger activity is a complex area and no more so when it comes to assessing, negotiating and agreeing upon the transfer, inheritance or retention of pension scheme liabilities. View online or download thermo scientific tsq quantum xls ultra user manual. The analytical precision of the hsrm assay was evaluated vs. Media backgrounder high level information for journalists thermo fisher scientific in mass spectrometry much of science is devoted to answering two questions.
Tsq quantum triple quadrupole system performs highly selective reaction monitoring hsrm analyzes complex samples quickly and efficiently. Feb 27, 2012 i have a tsq quantum xls in my lab, when i start the machine show me in the vacuum control windows the next mesage. Principal operator will be available during the installation certification period. Thermo fisher scientific, san jose, ca application note. One tsq quantum ultra triple quadrupole mass spectrometer thermofisher scientific, san. Quantification of complex samples using multiple reaction. A quantum rehab provider or a qualified technician must perform the initial setup of this power chair and must perform all of the procedures in this manual.
The tsq quantum ultra is a member of the tsq family of finnigan mass spectrometers. Overview to scale the picture below is a simulation at scale of the thermo tsq quantum access max lcms system mass spectrometer system right side connected with a dionex uhplc left side, installed on a ionbench ms mass spec bench or table. Ionmolecule adduct formation in tandem mass spectrometry. The thermo scientific tsq quantum am mass spectrometer is part of the thermo scientific family and is one of the only highresolution triple stage quadrupole mass spectrometers available that is particularly designed for accurate mass measurement. The jumper block is incorporated into the ide ata cable connector. Mar 14, 20 we have a tsq quantum ultra system and a tsq vantage system. Experimental a thermo scientific as 3000 ii autosampler and a thermo scientific trace gc ultra gas chromatograph, equipped with a backflush valve b. Then press the merge button to get your merged pdf. Tsq quantum access max tsq quantum ultra tsq vantage tsq quantum access. This device complies with low voltage directive 200695ec and harmonized standard en 610101. Overview to scale the picture below is a simulation at scale of the thermo tsq quantum ultra lcms system mass spectrometer system right side connected with a dionex uhplc left side, installed on a ionbench ms mass spec bench or table.
Welcome to the thermo electron, finnigan tsq quantum ultra system. Ionbench with the thermo tsq quantum access max mass. Recent advances in mass spectrometry for drug discovery and. Private equity group completes merger of top geospatial. Accurate mass data is generated on each of the 25 ions from 168 to 1224 da using the neighboring peaks as internal lock masses. Dryheat cooking of meats as a source of airborne n. Tsq quantum ultra triple quadrupole mass spectrometer quantify with outstanding accuracy using the thermo. Food safety, environmental, clinical, forensic, toxicology, pharmaceutical and. While techo is determined by linear physics, the time between the main merger event and the rst echo could be further a ected by nonlinear physics during merger, i. The residual samples were combined, and the mixture was evaporated using a centrifugation evaporator.
The formulation has been specifically optimized for use with the tsq endura series and tsq quantiva series instruments. Every effort has been made to supply complete and accurate information. The determination of anabolic steroids in human urine. Tsq quantum access max triple stage quadrupole mass. Triple quadrupole lcms thermo fisher scientific us. Our tsq triple quadrupole lcms systems enable targeted compound analysis for food safety, environmental, clinical research, and forensic toxicology laboratories. We have a tsq quantum ultra system and a tsq vantage system. Enhanced resolution triplequadrupole mass spectrometry for ultra sensitive and quantitative analysis of the investigational anticancer agent eo9 apaziquone and its metabolite eo5a in human and. Quantum unit of spin definition is a constant used as a unit of measurement for particle spin and equal to the planck constant divided by 2. The pierce triple quadrupole calibration solution, extended mass range, formulation contains 14 compounds that are ionizable in both positive and negative modes for instrument calibration. From targeted quantification to untargeted metabolomics. Problem with sensitivity of tsq quantumultra and tsq vantage. Thermo said that tsq vantage is higher sensitivity than tsq quantum ultra. System vented i tested leaks in the gc and detector i tested leaks in the column whe i go to help it show the next information.
Product specifications with the thermo scientific tsq quantum xls we continue the successful and wellknown tsq triple quadrupole mass spectrometer series, combined with the power, performance and flexibility of the thermo scientific trace gc ultra gas chromatograph. View brochure download pdf file lr, 4mb download pdf file hr, 29mb office. Tsq quantum xls ultra triple quadrupole gcms 8 the tsq quantum xls ultra triple quadrupole mass spectrometer addresses the requirements of the most demanding analytical tasks across applications. Quantitation of synthetic cannabinoids in urine using a.
Ionbench with the thermo tsq quantum ultra mass spectrometer. Equipnet is the worlds leading provider of used mass spectrometers and numerous other types of preowned equipment. The thermo scientific tsq quantum ultra mass spectrometer is part of the thermo scientific family and is one of the only high resolution triple stage quadrupole mass spectrometers available that is particularly designed for accurate mass measurement. Pdf a new methodology for targeted peptide quantitation in. This system features the innovative qedmsms scan mode for unmatched sens. Faims is a new tool, available on the tsq quantum ultra, for increasing lcms method selectivity. Low voltage safety compliance compliance with safety issues is declared under thermo fisher scientific sole responsibility. Sufficient bench space is available for all of the. This method provides broad drug coverage, fast turnaround time and is an excellent comparison to hydrolysis analysis. Using phytronixs laser diode thermal desorption technology ldtd it will also be possible to analyze any sample from any state gaseous, liquid or solid. Quantitation of synthetic cannabinoids in urine using a triple stage quadrupole lcms system in forensic toxicology kristine van natta, marta kozak. This tsq quantum ultra getting started manual provides you with information on how to set up, calibrate, and tune the tsq quantum ultra tsq quantum ultra.
The optimum temperature of operation is between 1821c 6570f. C, trpp1, and trpp2, photoinitiators bp and thbp, and pharmaceuticals phenacetin and levamisole were selected as model compounds and infused in lcq classic, tsq quantum ultra am, and qexactive orbitrap thermofisher scientific mass spectrometers using electrospray as ionization method. It is ideal for determination of masses in complex mixtures and quantitative analyses. Instrument method development workspace, showing an srm scan acquisition. Schematic of thermo qqq quantum ultra mass spectrometer equipped with dual ion. Overview to scale the picture below is a simulation at scale of the thermo tsq quantum access max lcms system mass spectrometer system right side connected with a dionex uhplc left side, installed on a. Benefits of the tsq quantum ultra include constant neutral loss scanning, parent scanning, highresolution precursor ion selectivity, srm and hsrm in order to deliver a complete solution for the proteomics and large molecule research community.
The room temperature may not change by more than 5c 9f during this period. Rapid analysis of opiates from low volume whole blood samples by lc msms utilizing turboflow methods author. New gctriple with ultra selective reaction monitoring. Finnigan tsq quantum discovery max thermofisher esi specification at 0. Tsq quantum ultra getting started version a thermo fisher. Tsq quantum xls emc directive 2004108ec emc compliance has been evaluated by tuv rheinland of north america inc. Donating products to help change the world the products we donate to organizations around the world benefit many causes, including. The tsq quantum xls delivers unsurpassed performance with superior.
Apci negative the measurement in the msms mode 2 transitions for bpa and c 12bpa each is listed in table 3. Applications such as pharmaceutical development, environmental and food safety testing, clinical research, and forensic toxicology demand analytical sensitivity and specificityeven when budgets are constrained. Tsq quantum access max triple quadrupole mass spectrometer. The maxtor fireball lct10 was developed by quantum corporation prior to its merger with maxtor.
It has a mass range of 101500 da without extended mass range electronic assemblies. Tsq quantum ultra ion max source introduced 1986 tsq 70 first fully computercontrolled tsq with hyperbolic quadrupoles 2005 tsq quantum ultra hesi introduced 1997 tsq 7000 api 2 interface 2000 tsq quantum first commercially available triple stage quadrupole with hsrm 0. Product specifications tsq quantum gc the next evolution. The determination of anabolic steroids in human urine using. L produces 27 ammoniated peg ions from 124 to 1268 da.
The symbols below are used throughout this owners manual and on the power chair to identify warnings and important information. Resolution up to 7,500 at mz 508 esi ionization mode. Find pricing on new and used thermo tsq quantum ultras and other mass spectrometers. Using the jumper pins you can establish the drive masterslave configuration. Analysis of microcystins from bluegreen algae using the. The thermo scientific tsq quantum access max triple stage quadrupole mass spectrometer is the valueconscious choice for a wide variety of applications, including pharmaceutical, environmental, food safety, clinical research, and forensics. However, when we determine amlodipine in human plasma by two those system after sample preparation with lle. Ltq ft ultratm tsq access maxtm tsq quantum discoverytm tsq quantum ultratm tsq vantagetm tsq enduratm tsq quantiva tm tsq altistm tsq quantistm tsq fortistm selection guide for thermo scientific mass spectrometers recommended not recommended tsqtm polytyrosine 1,3,6 ltq xl esitm positive ion calibration solution ltq velos esitm positive ion. Thermo fisher scientific launches new triple quadrupole. Measurement in the msms mode interface transition 1 target transition 2. Problem with sensitivity of tsq quantumultra and tsq.
This interface is installed in the atmospheric pressure region between the ion source and the mass spectrometer, allowing three complementary dimensions of separation to in the analysis. How to convert pdf to word without software duration. The virgin specimen a was firstly cut b, and then the broken halves were recombined for healing. Topoccasion thermo tsq quantum ultra lcmsms triple quad. The thermo scientific tsq quantum access max triple quadrupole mass spectrometer is an ou.
Lcms applications for food safety analysis cromlab. Finnigan tsq quantum hardware manual attachments finnigan tsq quantum hardware manual 4 mb. The stationary phase used was an acquity uplc hss c18 column 100 mm 2. We donated a thermo scientific tsq quantum ultra triple quadrupole mass spectrometer system and thermo scientific dionex ultimate 3000 uhplc system to students 2 science s2s. Tsq quatum xls and tsq quantum gc preinstallation requirement. This tsq quantum xls series user guide contains a description of the modes of operation and principle hardware components of your tsq quantum xls series system. Infusion of a mixture of polyethylene glycols pegs of average molecular weights 200,400, 600, and at 50 pmoles. Jul 17, 2012 thermo fisher scientific s triplequad line includes the tsq quantum access max, the tsq quantum ultra and the tsq vantage, with the latter offering the best sensitivity of the group.
Tsq vantage mass spectrometer shared resources fred. According to tichy, the access max, popular in the food and environmental safety industries, is the best priceperformance triple quad we offer, providing. The thermoelectron tsq vantage is a triple quadrupole mass spectrometer. T ptv injection port, thermo scientific trace gc ultra provided sample introduction into the tsq quantum xls mass spectrometer. The thermo scientific tsq quantum with esi source was designed to analyze gaseous samples using the apci mode. Enhanced resolution triplequadrupole mass spectrometry for. Used thermo finnigan tsq quantum ultra 3015768 mass spec. Enhanced sensitivity for selected reaction monitoring mass.
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